Contents
Preface
Introduction
Section 1 Purpose, requirements and rules of physical chemistry experiments
Section 2 Safety protection of physical chemistry experiments
Section 3 Errors and data processing in physical chemistry experiments
Section 4 Computer processing of physical chemistry experiment data
Combined experiment Ⅰ
Experiment 1 Determination of the heat of combustion of sucrose by constant volume thermal method
Experiment 2 Determination of the molar mass of sucrose by freezing point depression method
Experiment 3 Determination of the rate constant of the acid-catalyzed conversion reaction of sucrose by optical rotation method
Experiment 4 Determination of the Michaelis constant of sucrase by spectrophotometry
Combined experiment Ⅱ
Experiment 5 Determination of saturated vapor pressure of ethyl acetate by static method
Experiment 6 Evaporation and condensation method to draw the equilibrium phase diagram of ethyl acetate-ethanol two-liquid
system
Experiment 7 Determination of the rate constant and activation energy of ethyl saponification by conductivity method
Experiment 8 Determination of the dipole moment of ethyl acetate by the solution method
Combined experiment Ⅲ
Experiment 9 Determination of standard entropy and sublimation enthalpy of crystal iodine
Experiment 10 Determination of I2 distribution coefficient anddissociation constant
Experiment 11 Determination of the order of acetone iodization reactions
Experiment 12 “Iodine Clock” reaction
Combined experiment Ⅳ
Experiment 13 Determination of partial molar volume of NaCl
Experiment 14 Determination of osmotic pressure of NaCl injection
Experiment 15 Phase analysis of X-ray powder diffraction method of NaCl
Experiment 16 Drawing of three-component equilibrium phase diagram of KCl-HCl-H2O
Experiment 17 Determination of the heat of solution for KNO
Combined experiment Ⅴ
Experiment 18 Production and application of thermocouple
Experiment 19 Drawing of two-component metal phase diagram
Experiment 20 Determination of the electromotive potential of the original battery
Experiment 21 Surface modification and coloration of aluminum anodization
Experiment 22 Pyrophosphate copper plating
Experiment 23 Stainless steel electrolytic polishing and waste liquid treatment
Experiment 24 Synthesis, characterization and electrical properties of silver nano cables
Combined experiment Ⅵ
Experiment 25 Determination of surface tension of solution
Experiment 26 Determination of critical micelle concentration of surfactants
Experiment 27 Preparation and stability of sol
Experiment 28 Determination of sol electric potential
Experiment 29 Preparation and properties of emulsion
Experiment 30 Determination of the average molar mass of polymer compounds
Combined experiment Ⅶ
Experiment 31 Determination of magnetic susceptibility
Experiment 32 Biomineral and biomineralization
Experiment 33 Synthesis and structure analysis of KDP crystals
Experiment 34 Molecular model and crystal structure
References
Appendix 1 Special topic of physical chemistry experiment technology
Special Topic Ⅰ Temperature measurement technology and instruments
Special Topic Ⅱ Pressure measurement technology and instruments
Special Topic Ⅲ Density measurement technology and instruments
Special Topic Ⅳ Electrical measurement technology and instruments
Special Topic Ⅴ Optical measurement technology and instruments
Special Topic Ⅵ Viscosity measurement technology and instruments
Appendix 2 Data sheets commonly used in physical chemistry experiments