Part 1 Experimental Organic Chemistry Chapter 1 General Introduction 3
1. Laboratory Rules. 3
2. Safety Rules and Regulations in Chemistry Laboratory . 3
3. Treatment of the Common Accidents in Laboratory. 5
4. Fire Prevention and Treatment . 5
5. First Aid Kit 5
6. Preview, Record and Laboratory Report. 5
Chapter 2 Common laboratory Apparatus and Equipment . 7
1. General Glassware 7
2. Common Standard-taper Glassware 7
3. Common Glass Apparatus. 8
4. Common Equipment 8
Chapter 3 Laboratory Experiments 11
Experiment 1 Basic Laboratory Techniques (Ⅰ) . 11
Experiment 2 Basic Laboratory Techniques (Ⅱ) . 14
Experiment 3 Extraction of Iodine. 16
Experiment 4 Determination of the Melting Point 18
Experiment 5 Micro Determination of the Boiling Point 19
Experiment 6 Refractive Index Determination of Liquid Organic Compound 21
Experiment 7 Operation of Organic Molecular Models. 23
Experiment 8 Paper Electrophoresis of Amino Acid 25
Experiment 9 Column Chromatography 27
Experiment 10 Thin-Layer Chromatography (TLC) . 29
Experiment 11 Paper Chromatography 31
Experiment 12 Preparation of Aspirin 34
Experiment 13 Preparation of Acetanilide . 36
Experiment 14 Extraction of Rutin and Recovery of Extraction Agent 38
Experiment 15 Analysis of Unknown Sample of Organic Compounds (Designing Experiment). 39
Part 2 Solutions Manual for Organic Chemistry
Chapter Introduction 43
Chapter Saturated Hydrocarbons: Alkanes and Cycloalkanes . 45
Chapter Unsaturated Hydrocarbons: Alkenes, Alkynes and Aromatics. 48
Chapter Alcohols, Phenols, and Ethers 51
Chapter Aldehydes and Ketones . 55
Chapter Carboxylic Acids and Acid Derivatives. 59
Chapter Amines . 64
Chapter Optical Isomerism 66
Chapter Carbohydrate. 70
Chapter Lipids. 73
Chapter Proteins . 76
Chapter Nucleic Acids 79
References 80